N-Methylbenzylamine → HCID 22981193, compound

HRID 1861973Notes

Reaction equation

[C:1]([O:5][C:6]([N:8]([C:20]([O:22][C:23]([CH3:26])([CH3:25])[CH3:24])=[O:21])[CH2:9][C:10]1[CH:15]=[C:14]([N+:16]([O-:18])=[O:17])[CH:13]=[CH:12][C:11]=1F)=[O:7])([CH3:4])([CH3:3])[CH3:2].[CH3:27][NH:28][CH2:29][C:30]1[CH:35]=[CH:34][CH:33]=[CH:32][CH:31]=1>>[C:1]([O:5][C:6]([N:8]([C:20]([O:22][C:23]([CH3:26])([CH3:25])[CH3:24])=[O:21])[CH2:9][C:10]1[CH:15]=[C:14]([N+:16]([O-:18])=[O:17])[CH:13]=[CH:12][C:11]=1[N:28]([CH2:29][C:30]1[CH:35]=[CH:34][CH:33]=[CH:32][CH:31]=1)[CH3:27])=[O:7])([CH3:4])([CH3:3])[CH3:2]

Participants

Reactant 2

HCID 7669N-Methylbenzylamine

HCID 22981229HCID 22981229, compound

Product 1

HCID 22981193HCID 22981193, compoundYield 56%

Procedure

Using the compound obtained in Example 263 as a starting material and also using N-methylbenzylamine as a reagent, the same procedure of Example 264 gave the titled compound (yield, 56%).

Sources & evidence

ORD record: ord-fd5b52b7700c406e9a6c1e5d96fb793c
Source dataset: uspto-grants-2003_03
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06534546B1

Reaction notes

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