3,5-Dibromosalicylaldehyde → HCID 135450066, compound

HRID 1862382Notes

Reaction equation

HRID 1862382 reaction equation
[CH3:1][C:2]1([CH3:10])[CH2:7][CH2:6][C:5](=O)[CH2:4][C:3]1=[O:9].[Br:11][C:12]1[C:13]([OH:21])=[C:14]([CH:17]=[C:18]([Br:20])[CH:19]=1)[CH:15]=O.[NH2:22][C:23]1[CH:27]=[CH:26][NH:25][N:24]=1>>[Br:11][C:12]1[C:13]([OH:21])=[C:14]([CH:15]2[C:4]3[C:3](=[O:9])[C:2]([CH3:10])([CH3:1])[CH2:7][CH2:6][C:5]=3[NH:22][C:23]3=[CH:27][CH:26]=[N:25][N:24]23)[CH:17]=[C:18]([Br:20])[CH:19]=1

Participants

4

Reactant 3

HCID 70243,5-DibromosalicylaldehydeHCID 1363601,3-Cyclohexanedione, 4,4-dimethyl-HCID 178418806HCID 178418806, compound

Product 1

HCID 135450066HCID 135450066, compound

Procedure

4,4-Dimethyl-1,3-cyclohexanedione, 3,5-dibromo-2-hydroxybenzaldehyde and 3-aminopyrazole were processed as described in General Procedure A to provide the title compound.

Sources & evidence

ORD record
ord-21572e4c111e47a591d40c600375eb9f
Source dataset
uspto-grants-2003_03
Patent number
US06538000B1

Reaction notes

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