HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-bromobutanimide → HCID 135449959, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | HCID 135494158 | HCID 135494158 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 135449959 | HCID 135449959 | 83.8% |
Reaction Steps
The product from Example 6 (0.52 g, 1.56 mmol) in dichloromethane was treated with N-bromosuccinimide (0.28 mg, 1.56 mmol) and allowed to stir at ambient temperature overnight. The mixture was filtered and the filter cake washed with CH2Cl2 to provide the title compound (0.54 g) as a solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06538000B1 |
| Source dataset | uspto-grants-2003_03 |
| ORD ID | ord-6404f7be25d04e4f97fc77cd3c49b62c |
| Source note | uspto-grants-2003_03 |