HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18620099, compound → HCID 18620128, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18620099 | HCID 18620099 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 18620128 | HCID 18620128 | 100.1% |
Reaction Steps
To a solution of 2-benzyloxy-5-(2-methoxymethoxyethyl)benzonitrile (711 mg) in ethyl acetate (10 ml) was added 10% palladium carbon (100 mg), and the mixture was stirred for 30 minutes at room temperature under a hydrogen atmosphere. After removal of the catalyst by filtration, removal of the solvent under reduced pressure gave 2-hydroxy-5-(2-methoxymethoxyethyl)benzonitrile (496 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06538152B1 |
| Source dataset | uspto-grants-2003_03 |
| ORD ID | ord-a7da5b3e98624f869579df5188a49cd8 |
| Source note | uspto-grants-2003_03 |