HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 70007150, compound → HCID 10165003, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 70007150 | HCID 70007150 | — |
| Solvent | Chloroform methanol | HCID 21584188 | — |
| Product | HCID 10165003 | HCID 10165003 | 87.8% |
Reaction Steps
N-{2-[4-(2-{[(2S)-3-(4-{[tert-Butyl(diphenyl)silyl]oxy}phenoxy)-2-hydroxypropyl]amino}ethyl)anilino]-3-pyridinyl}-N′-hexylurea (0.15 g, 0.197 mmol) was reacted according to Procedure H (eluant: 10:1 going to 5:1 chloroform-methanol containing 2% triethylamine) to give the title compound (0.09 g, 0.173 mmol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06537994B2 |
| Source dataset | uspto-grants-2003_03 |
| ORD ID | ord-8971a21600b245d0bed16697cd263dbd |
| Source note | uspto-grants-2003_03 |