HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 70007043, compound → HCID 70008383, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 70007043 | HCID 70007043 | — |
| Solvent | Chloroform methanol | HCID 21584188 | — |
| Product | HCID 70008383 | HCID 70008383 | 86% |
Reaction Steps
3-[4-(2-{[(2S)-3-(4-{[tert-Butyl(diphenyl)silyl]oxy}phenoxy)-2-hydroxypropyl]amino}ethyl)phenyl]-1-isopropenyl-1,3-dihydro-2H-imidazo[4,5-b]pyridin-2-one (0.19 g, 0.272 mmol) was reacted according to Procedure H (eluant: 10:1 going to 5:1 chloroform-methanol containing 2% triethylamine) to give the title compound (0.108 g, 0.234 mmol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06537994B2 |
| Source dataset | uspto-grants-2003_03 |
| ORD ID | ord-2042de9e9d044d70b0ecc1d736a6245b |
| Source note | uspto-grants-2003_03 |