HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tert-butyl-(4-oxiranylmethoxy-phenoxy)-diphenylsilane → HCID 12045568, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tert-butyl-(4-oxiranylmethoxy-phenoxy)-diphenylsilane | HCID 12045564 | — |
| Reactant | HCID 18619656 | HCID 18619656 | — |
| Solvent | Chloroform methanol | HCID 21584188 | — |
| Product | HCID 12045568 | HCID 12045568 | 42.6% |
Reaction Steps
4-[2-(4-Cyclohexylphenyl)-3H-imidazo[4,5-b]pyridin-3-yl]phenethylamine (0.37 g, 0.93 mmol) was reacted with tert-butyl-(4-oxiranylmethoxy-phenoxy)-diphenyl-silane (0.377 g, 0.93 mmol) according to Procedure G (eluant: 20:1 going to 5:1 chloroform-methanol) to give the title compound (0.317 g, 0.396 mmol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06537994B2 |
| Source dataset | uspto-grants-2003_03 |
| ORD ID | ord-60361438c4c3499ebc76fd9266dd1e8f |
| Source note | uspto-grants-2003_03 |