HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 70007667, compound → HCID 18619640, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 70007667 | HCID 70007667 | — |
| Solvent | Chloroform methanol | HCID 21584188 | — |
| Product | HCID 18619640 | HCID 18619640 | 49.1% |
Reaction Steps
N-(3-{3-[4-(2-{[(2S)-3-(4-{[tert-butyl(diphenyl)silyl]oxy}phenoxy)-2-hydroxypropyl]amino}ethyl)phenyl]-3H-imidazo[4,5-b]pyridin-2-yl}phenyl)-N′-hexylurea (0.19 g, 0.22 mmol) was reacted according to Procedure H (eluant: 10:1 going to 5:1 chloroform-methanol containing 1% ammonium hydroxide) to give the title compound (0.067 g, 0.108 mmol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06537994B2 |
| Source dataset | uspto-grants-2003_03 |
| ORD ID | ord-e44e1f1503b446eabccd05629654a8e9 |
| Source note | uspto-grants-2003_03 |