HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 70007497, compound → HCID 70007134, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 70007497 | HCID 70007497 | — |
| Solvent | Chloroform methanol | HCID 21584188 | — |
| Product | HCID 70007134 | HCID 70007134 | 89.5% |
Reaction Steps
N-[4-(2-{3-[4-(2-{[(2S)-3-(4-{[tert-Butyl(diphenyl)silyl]oxy}phenoxy)-2-hydroxypropyl]amino}ethyl)phenyl]-3H-imidazo[4,5-b]pyridin-2-yl}ethyl)phenyl]-N′-hexylurea (0.195 g, 0.220 mmol) was reacted according to Procedure H (eluant: 10:1 going to 5:1 chloroform-methanol containing 1% ammonium hydroxide) to give the title compound (0.128 g, 0.197 mmol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06537994B2 |
| Source dataset | uspto-grants-2003_03 |
| ORD ID | ord-75d7078aab704e5bade68ba6c8a4d63c |
| Source note | uspto-grants-2003_03 |