HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bisphenol A diglycidyl ether → HCID 20393558, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bisphenol A diglycidyl ether | HCID 2286 | — |
| Reactant | 4-Amino-1,2,2,6,6-pentamethylpiperidine | HCID 693792 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 20393558 | HCID 20393558 | — |
Reaction Steps
To 100 ml of methanol were added 12 g of 4-amino-1,2,2,6,6-pentamethylpiperidine and 11 g of 2,2-bis[p-(2,3-epoxypropoxy)phenyl]propane; the mixture was then reacted in a similar manner to that described in Example 1, giving the desired compound in the form of white crystals melting at 141°-143° C. The compound had an Rf value of 0.64 on thin layer chromatography on silica gel developed with a 1:3:1 by volume mixture of methanol, ethyl acetate and triethylamine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04166813 |
| Source dataset | uspto-grants-1979_09 |
| ORD ID | ord-4d00d188fb9d4d29be2cde2285d8b9d1 |
| Source note | uspto-grants-1979_09 |