HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → 5-Nitroso-2,4,6-pyrimidinetriamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | 2,4,6-Triaminopyrimidine | HCID 13863 | — |
| Reactant | Sodium Nitrite | HCID 23668193 | — |
| Solvent | Water | HCID 962 | — |
| Product | 5-Nitroso-2,4,6-pyrimidinetriamine | HCID 70504 | — |
Reaction Steps
2,4,6-triamino-5-nitrosopyrimidine was prepared by dissolving 1.0 mole of 2,4,6-triaminopyrimidine in 1040 ml of water and 1.5 moles of acetic acid, maintaining the temperature in the range of about 0°-16° C. Then 1.0 mole of sodium nitrite was added to the reaction mixture while controlling the reaction temperature in the range of 0°-20° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04167633 |
| Source dataset | uspto-grants-1979_09 |
| ORD ID | ord-bb38db780a59447da987a7f2eca89566 |
| Source note | uspto-grants-1979_09 |