HRID1863112

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID6570

Methyl vinyl ketone

C4H6O

HCID4653152

4,5-dimethoxy-2-nitroaniline

C8H10N2O4

PRODUCTS

生成物

HCID619108

未命名化合物

收率 27%

PROCEDURE

实验过程

A Skraup reaction of 4,5 -dimethoxy-2-nitroaniline with methyl vinyl ketone gave a 27% yield of 5,6-dimethoxy-4-methyl-8-nitroquinoline. The yellow compound crystallized well from methanol; mp 126°-127.5°.