HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 20393446, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Sulfuric acid magnesium salt (1:1) | HCID 24083 | — |
| Reactant | 64993-13-1 | HCID 432307 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 20393446 | HCID 20393446 | — |
Reaction Steps
A solution of 28.1 g (0.0779 mole) of 8-(6-diethylaminohexylamino)-5-fluoro-6-methoxy-4-methylquinoline in ether (1.0 l) was dried over anhydrous magnesium sulfate then saturated with anhydrous hydrogen chloride. The gummy solid which separated was collected then recrystallized from ethanol-ether (2:5) (1.4 l); yield 27.3 g (80.8% recovery); mp 263°-269°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04167638 |
| Source dataset | uspto-grants-1979_09 |
| ORD ID | ord-f84f47a7ae294c9f87e6d0b1354811d6 |
| Source note | uspto-grants-1979_09 |