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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1863209Erstellt: 25. Oktober 2026

Dimethylcarbamoyl Chloride → 2-Methyl-4-dimethylaminocarbonyloxyquinoline

https://huagongshe.com/reaction/1863209

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktDimethylcarbamoyl ChlorideHCID 6598—
Edukt2-Methylquinolin-4-olHCID 178428811—
LösungsmittelDimethylformamideHCID 6228—
Produkt2-Methyl-4-dimethylaminocarbonyloxyquinolineHCID 12798236—

Reaktionsschritte

24 g (0,15 mole) of 2-methyl-4-hydroxyquinoline were dissolved in 200 ml of dimethylformamide (anhydrous and free from amine), 23 g (0,22 mole) of triethylmine were added and, subsequently, 24 g (0,22 mole) of dimethylcarbamic acid chloride added dropwise.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04168311
Quelldatensatzuspto-grants-1979_09
ORD IDord-eee3b64759c04749bf65c8b2db11902e
Quellennotizuspto-grants-1979_09