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HRID1863209

反应详情

EQUATION

反应方程式

HRID 1863209 的结构方程式

REACTANTS

反应物

2
结构：CN(C)C(=O)Cl
HCID6598

Dimethylcarbamoyl chloride

C3H6ClNO

结构：Cc1cc(O)c2ccccc2n1
HCID178428811

未命名化合物

PRODUCTS

生成物

1
结构：Cc1cc(OC(=O)N(C)C)c2ccccc2n1
HCID12798236

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CN(C)C=O
溶剂HCID6228

N,N-Dimethylformamide

C3H7NO

PROCEDURE

实验过程

24 g (0,15 mole) of 2-methyl-4-hydroxyquinoline were dissolved in 200 ml of dimethylformamide (anhydrous and free from amine), 23 g (0,22 mole) of triethylmine were added and, subsequently, 24 g (0,22 mole) of dimethylcarbamic acid chloride added dropwise.

WORKUP

后处理

  1. addition23 g (0,22 mole) of triethylmine were added