HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 54026503, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | HCID 53870913 | HCID 53870913 | — |
| Catalyst | Silver(II) oxide | HCID 92152 | — |
| Product | HCID 54026503 | HCID 54026503 | 82.6% |
Reaction Steps
A mixture of 5.0 g of 1-bromotricyclo[4.3.1.12,5 ]undecane, 3.0 g of silver oxide and 30 ml of anhydrous ethanol was refluxed for 2 hours. Thereafter, the mixture was treated in the same manner as described in Example 1 to obtain 3.5 g (yield, 82.6%) of 1-ethoxytricyclo[4.3.1.12,5 ]undecane having a boiling point of 97° to 98° C./4 mmHg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04168389 |
| Source dataset | uspto-grants-1979_09 |
| ORD ID | ord-9946ae2a1de5456388350768be1db056 |
| Source note | uspto-grants-1979_09 |