HRID1863243
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
A mixture of 5.0 g of 1-bromotricyclo[4.3.1.12,5 ]undecane, 3.0 g of silver oxide and 30 ml of anhydrous ethanol was refluxed for 2 hours. Thereafter, the mixture was treated in the same manner as described in Example 1 to obtain 3.5 g (yield, 82.6%) of 1-ethoxytricyclo[4.3.1.12,5 ]undecane having a boiling point of 97° to 98° C./4 mmHg.
WORKUP
后处理
- temperaturewas refluxed for 2 hours
- additionThereafter, the mixture was treated in the same manner