HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Butanol → HCID 54230553, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Butanol | HCID 263 | — |
| Reactant | HCID 53870913 | HCID 53870913 | — |
| Catalyst | Silver(II) oxide | HCID 92152 | — |
| Product | HCID 54230553 | HCID 54230553 | 65.3% |
Reaction Steps
A mixture of 3.0 g of 1-bromotricyclo[4.3.1.12,5 ]undecane, 2.0 g of silver oxide and 30 ml of anhydrous n-butanol was refluxed for 6 hours. Thereafter, the mixture was treated in the same manner as described in Example 1, and there was obtained 1.9 g (yield, 65.3%) of 1-n-butoxytricyclo[4.3.1.12,5 ]undecane having a boiling point of 97° to 98° C./1 mmHg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04168389 |
| Source dataset | uspto-grants-1979_09 |
| ORD ID | ord-12399872208345199112f99374286035 |
| Source note | uspto-grants-1979_09 |