HRID1863244

反应详情

EQUATION

反应方程式

HRID 1863244 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

A mixture of 3.0 g of 1-bromotricyclo[4.3.1.12,5 ]undecane, 2.0 g of silver oxide and 30 ml of anhydrous n-butanol was refluxed for 6 hours. Thereafter, the mixture was treated in the same manner as described in Example 1, and there was obtained 1.9 g (yield, 65.3%) of 1-n-butoxytricyclo[4.3.1.12,5 ]undecane having a boiling point of 97° to 98° C./1 mmHg.

WORKUP

后处理

  1. temperaturewas refluxed for 6 hours
  2. additionThereafter, the mixture was treated in the same manner