HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Chlorothiophenol → HCID 20392578, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Chlorothiophenol | HCID 7815 | — |
| Reactant | HCID 20392609 | HCID 20392609 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 20392578 | HCID 20392578 | — |
Reaction Steps
Methyl α-bromo-α-[p-(phenoxy)phenyl]acetate (6.42 g) is reacted with 3.61 g of 4-chlorothiophenol in methanol as in Example 16 to afford a yellow oil which solidifies on standing. Recrystallization from 50 ml of petroleum ether affords the product as white crystals, mp 66°-67.5° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04168385 |
| Source dataset | uspto-grants-1979_09 |
| ORD ID | ord-fb4d791c888c4b64aa67498e82df0ec7 |
| Source note | uspto-grants-1979_09 |