HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Hydroxide → HCID 20392599, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | HCID 20392578 | HCID 20392578 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 20392599 | HCID 20392599 | — |
Reaction Steps
A mixture of 3.55 g of methyl α-(p-chlorophenylthio)-α-[p-(phenoxy)phenyl]acetate, 20 ml of 20% KOH and 5 ml of methanol is refluxed overnight. The mixture is acidified and worked up to afford a light green solid which is crystallized from chloroform to yield the product as white crystals, mp 121°-125° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04168385 |
| Source dataset | uspto-grants-1979_09 |
| ORD ID | ord-83ddf36a99594f52a04681272702f7f2 |
| Source note | uspto-grants-1979_09 |