反应详情

In a manner similar to Example 16, 7.62 g of methyl α-bromo-α-[p-(α,α,α-trifluoro-m-tolyloxy)phenyl]acetate was reacted with 3.21 g of p-chlorophenol to give a gel which crystallized on trituration with 50 ml of petroleum ether (6.45 g). Recrystallization from 50 ml of hexane yielded a 5.8 g of a white solid, mp 79°-82° C.

1. customto give a gel which
2. customcrystallized on trituration with 50 ml of petroleum ether (6.45 g)
3. customRecrystallization from 50 ml of hexane