HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 178494684, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | Dihydroxyacetone | HCID 670 | — |
| Reactant | Ethyl 2-methoxyethanecarboximidate hydrochloride | HCID 12816254 | — |
| Product | HCID 178494684 | HCID 178494684 | — |
Reaction Steps
A 307.2 gm. portion of ethyl 2-methoxyacetimidate hydrochloride [Rule, J. Chem. Soc. 113, 9 (1918)] and 180 gm. of 1,3-dihydroxyacetone in one liter of liquid ammonia are reacted as described in Example 3 giving the desired product as an oil. A crystalline picrate salt (m.p. 175°-178° C.) is obtained by heating the oily product and picric acid in water.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04168964 |
| Source dataset | uspto-grants-1979_09 |
| ORD ID | ord-d4eb8d81ffe94f3588f8f363095c3347 |
| Source note | uspto-grants-1979_09 |