Ethanol → HCID 178473581, compound

HRID 1863388Notes

Reaction equation

HRID 1863388 reaction equation
[C:1]([O:5][CH2:6][CH3:7])(=[O:4])[NH:2][NH2:3].C(O)C.[CH3:11][C:12]1[NH:13][CH:14]=[C:15]([CH:17]=O)[N:16]=1>C(O)C.C(O)(=O)C>[CH2:6]([O:5][C:1](=[O:4])[NH:2][N:3]=[CH:17][C:15]1[N:16]=[C:12]([CH3:11])[NH:13][CH:14]=1)[CH3:7]

Participants

6

Reactant 3

HCID 702EthanolHCID 20064Hydrazinecarboxylic acid, ethyl esterHCID 178418999HCID 178418999, compound

Product 1

HCID 178473581HCID 178473581, compound

Reagents, catalysts & solvents 2

HCID 702EthanolCatalystHCID 176Acetic AcidSolvent

Procedure

A solution of 16.68 gm. of ethyl carbazate in 50 ml. of hot ethanol is added to a solution of 16.50 gm. of 2-methyl-4-imidazolecarboxaldehyde in 100 ml. of hot ethanol containing 2 drops of acetic acid. The reaction is carried out as described in Example 32 giving the desired product, m.p. 210.5°-211.5° C.

Sources & evidence

ORD record
ord-03685b62875f469283cd0b85c6fde76b
Source dataset
uspto-grants-1979_09
Patent number
US04168964

Reaction notes

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