HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 178473581, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Hydrazinecarboxylic acid, ethyl ester | HCID 20064 | — |
| Reactant | HCID 178418999 | HCID 178418999 | — |
| Catalyst | Ethanol | HCID 702 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 178473581 | HCID 178473581 | — |
Reaction Steps
A solution of 16.68 gm. of ethyl carbazate in 50 ml. of hot ethanol is added to a solution of 16.50 gm. of 2-methyl-4-imidazolecarboxaldehyde in 100 ml. of hot ethanol containing 2 drops of acetic acid. The reaction is carried out as described in Example 32 giving the desired product, m.p. 210.5°-211.5° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04168964 |
| Source dataset | uspto-grants-1979_09 |
| ORD ID | ord-03685b62875f469283cd0b85c6fde76b |
| Source note | uspto-grants-1979_09 |