Diphenyl Ether → HCID 13548755, compound

HRID 1863400Notes

Reaction equation

HRID 1863400 reaction equation
C[S:2][C:3](=S)[NH:4][N:5]=[CH:6][C:7]1[N:8]=[C:9]([CH3:13])[NH:10][C:11]=1[CH3:12].C1(OC2C=CC=CC=2)C=CC=CC=1>>[CH3:13][C:9]1[N:8]2[C:3](=[S:2])[NH:4][N:5]=[CH:6][C:7]2=[C:11]([CH3:12])[N:10]=1

Participants

3

Reactant 2

HCID 7583Diphenyl EtherHCID 136002961HCID 136002961, compound

Product 1

HCID 13548755HCID 13548755, compound

Procedure

A mixture of 30.26 gm. of 3-[(2,5-dimethyl-4-imidazolyl)methylene]dithiocarbazic acid methyl ester and 125 ml. of diphenyl ether is reacted as described in Example 58 giving a solid which is the desired product, m.p. 287.5°-290° C.

Workup

  1. additionA mixture of 30.26 gm

Sources & evidence

ORD record
ord-ffe711ebe3174648a7a02ad3798d994c
Source dataset
uspto-grants-1979_09
Patent number
US04168964

Reaction notes

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