Diphenyl Ether → HCID 12493301, compound

HRID 1863402Notes

Reaction equation

HRID 1863402 reaction equation
C[S:2][C:3](=S)[NH:4][N:5]=[CH:6][C:7]1[N:8]=[C:9]([CH2:13][CH2:14][CH3:15])[NH:10][C:11]=1[CH3:12].C1(OC2C=CC=CC=2)C=CC=CC=1>>[CH3:12][C:11]1[N:10]=[C:9]([CH2:13][CH2:14][CH3:15])[N:8]2[C:7]=1[CH:6]=[N:5][NH:4][C:3]2=[S:2]

Participants

3

Reactant 2

HCID 7583Diphenyl EtherHCID 136098647HCID 136098647, compound

Product 1

HCID 12493301HCID 12493301, compound

Procedure

A mixture of 32.12 gm. of 3-[(5-methyl-2-n-propyl-4-imidazolyl)methylene]dithiocarbazic acid methyl ester and 200 ml. of diphenyl ether is reacted as described in Example 58 giving the desired product, m.p. 183°-186° C.

Workup

  1. additionA mixture of 32.12 gm

Sources & evidence

ORD record
ord-a1558387388f4892a5bb5c3140b24812
Source dataset
uspto-grants-1979_09
Patent number
US04168964

Reaction notes

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