Diphenyl Ether → HCID 12493300, compound

HRID 1863404Notes

Reaction equation

HRID 1863404 reaction equation
C[S:2][C:3](=S)[NH:4][N:5]=[CH:6][C:7]1[N:8]=[C:9]([CH2:12][O:13][CH3:14])[NH:10][CH:11]=1.C1(OC2C=CC=CC=2)C=CC=CC=1>>[CH3:14][O:13][CH2:12][C:9]1[N:8]2[C:3](=[S:2])[NH:4][N:5]=[CH:6][C:7]2=[CH:11][N:10]=1

Participants

3

Reactant 2

HCID 7583Diphenyl EtherHCID 178494682HCID 178494682, compound

Product 1

HCID 12493300HCID 12493300, compound

Procedure

A mixture of 62.4 gm. of 3-{[2-(methoxymethyl)-4-imidazolyl]methylene}dithiocarbazic acid methyl ester and 250 ml. of diphenyl ether is reacted as described in Example 58 giving the desired product m.p. 219.5°-223° C.

Workup

  1. additionA mixture of 62.4 gm

Sources & evidence

ORD record
ord-73e4c8f8cca04cafb02ebecd05cf6c57
Source dataset
uspto-grants-1979_09
Patent number
US04168964

Reaction notes

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