Diphenyl Ether → HCID 12493304, compound
Reaction equation
C([O:3][C:4](=O)[NH:5][N:6]=[CH:7][C:8]1[N:9]=[C:10]([C:13]([CH3:16])([CH3:15])[CH3:14])[NH:11][CH:12]=1)C.C1(OC2C=CC=CC=2)C=CC=CC=1>>[C:13]([C:10]1[N:9]2[C:4](=[O:3])[NH:5][N:6]=[CH:7][C:8]2=[CH:12][N:11]=1)([CH3:16])([CH3:15])[CH3:14]Participants
3
Procedure
A 6.15 gm. portion of 3-(2-tert-butyl-4-imidazolylmethylene)carbazic acid ethyl ester in 40 ml. of diphenyl ether is reacted as described in Example 70 giving the desired product, m.p. 186°-188° C.
Sources & evidence
- ORD record
- ord-c76cd4048250418e954727fb69258e14
- Source dataset
- uspto-grants-1979_09
- Patent number
- US04168964
Reaction notes
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