Diphenyl Ether → HCID 13548685, compound
Reaction equation
C([O:3][C:4](=O)[NH:5][N:6]=[CH:7][C:8]1[N:9]=[CH:10][NH:11][C:12]=1[CH3:13])C.C1(OC2C=CC=CC=2)C=CC=CC=1>>[CH3:13][C:12]1[N:11]=[CH:10][N:9]2[C:8]=1[CH:7]=[N:6][NH:5][C:4]2=[O:3]Participants
3
Procedure
A mixture of 10.26 gm. of 3-(5-methyl-4-imidazolylmethylene)carbazic acid ethyl ester and 100 ml. of diphenyl ether is reacted as described in Example 70 giving the desired product, m.p. 276°-282° C.
Workup
- additionA mixture of 10.26 gm
Sources & evidence
- ORD record
- ord-a1108054fab243c3bdfd16a763a43d12
- Source dataset
- uspto-grants-1979_09
- Patent number
- US04168964
Reaction notes
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