HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl carbazate → HCID 136398811, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl carbazate | HCID 80519 | — |
| Reactant | 1-(5-methyl-2-phenyl-1H-imidazol-4-yl)ethan-1-one | HCID 328820 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 136398811 | HCID 136398811 | — |
Reaction Steps
Methyl 5-methyl-2-phenyl-4-imidazolyl ketone (4.5 gm., 0.023 mole) is refluxed with methyl carbazate (2.4 gm., 0.023 mole) in toluene (112 ml.) for 5 hours. The toluene is removed, and the solid washed with water (3×50 ml.). The solid is recrystallized from methanol to yield the product (1.28 gm., 20.9%), m.p. 201°-201.5° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04168964 |
| Source dataset | uspto-grants-1979_09 |
| ORD ID | ord-bcd2f286c8f24d85ade10422601effc7 |
| Source note | uspto-grants-1979_09 |