HuagongsheHuagongshe Chemistry Print Report · For research reference only
Glycine xylidide → HCID 13177105, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Glycine xylidide | HCID 87833 | — |
| Reactant | Ethanimidic acid, ethyl ester, hydrochloride (1:1) | HCID 2724290 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 13177105 | HCID 13177105 | — |
Reaction Steps
4.85 Grams (0.039 mole) of ethyl acetimidate hydrochloride and 7.0 g of 2-amino-2',6'-dimethylacetanilide were dissolved in 75 ml of anhydrous ethanol and stirred at room temperature for two days. The solid which formed was collected on a filter, recrystallized from ethanol, and dried overnight under vacuum at 60° C. M.P. 240°-241° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04169106 |
| Source dataset | uspto-grants-1979_09 |
| ORD ID | ord-7f6e5176ec1940ddaf0cc34a1f3cf344 |
| Source note | uspto-grants-1979_09 |