Hydrazine → HCID 57973798, compound

Participants

Reaction Steps

A mixture of 132 mg (0.6 mmol) of 4-chloro-2-(trifluoromethyl)-1H-imidazo[4,5-c]pyridine, 0.0787 mL (2.4 mmol) of anhydrous hydrazine, and 3 mL of ethanol was stirred at reflux for 2 days. The cooled, filtered solution was concentrated, and the residue was partitioned between ethyl acetate and water. The organic phase was dried over sodium sulfate, filtered and concentrated to yield the title compound. LC-MS 218 (M+1).

Provenance & Evidence