HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,2-Dimethylethenylboronic acid → HCID 131727806, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,2-Dimethylethenylboronic acid | HCID 2763299 | — |
| Reactant | HCID 131727795 | HCID 131727795 | — |
| Solvent | Dichloromethane methanol | HCID 21226129 | — |
| Product | HCID 131727806 | HCID 131727806 | — |
Reaction Steps
The titled compound was prepared according to general method D by reaction of rac-3-[cis-2,3-bis-(4-chloro-phenyl)-5-oxo-2,3-dihydro-6-iodo-5H-imidazo[1,2-a]pyridine-1-sulfonyl]-benzonitrile with 2,2-dimethylethenylboronic acid. The compound was isolated by FCC (2.5% MeOH/DCM). The expected product was characterized by 1H NMR
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07625895B2 |
| Source dataset | uspto-grants-2009_12 |
| ORD ID | ord-af7cab8b2be848bba0c76e5b9e70cfd6 |
| Source note | uspto-grants-2009_12 |