HuagongsheHuagongshe Chemistry Print Report · For research reference only
Morpholine → HCID 131727807, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Morpholine | HCID 8083 | — |
| Reactant | HCID 131727808 | HCID 131727808 | — |
| Product | HCID 131727807 | HCID 131727807 | — |
Reaction Steps
rac-3-[cis-2,3-Bis-(4-chloro-phenyl)-6-morpholin-4-ylmethyl-5-oxo-2,3-dihydro-5H-imidazo[1,2-a]pyridine-1-sulfonyl]-benzonitrile was prepared according to general method E by reaction of rac-3-[cis-2,3-bis-(4-chloro-phenyl)-6-formyl-5-oxo-2,3-dihydro-5H-imidazo[1,2-a]pyridine-1-sulfonyl]-benzonitrile with Morpholine. The compound was isolated by preparative HPLC. The expected product was characterized by LC/MS (M+H) where the mass was observed as 621.06; the expected mass is 620. LC/MS indicated a purity of 100% as measured by UV 214 nM.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07625895B2 |
| Source dataset | uspto-grants-2009_12 |
| ORD ID | ord-4dc3f166925045c2b9bef84e8e92c6f4 |
| Source note | uspto-grants-2009_12 |