HRID1864511

反应详情

EQUATION

反应方程式

HRID 1864511 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

A solution of N-[1-(diphenylmethyl)-3-azetidinyl]-methanesulfonamide (185 mg, 0.585 mmol) in MeOH (10 mL) was treated with 1 mL of 4.0 N HCl/dioxane and then reacted overnight with hydrogen gas at 50 psi. The reaction mixture was then filtered through a pad of Celite and used without further purification.

WORKUP

后处理

  1. filtrationThe reaction mixture was then filtered through a pad of Celite
  2. customused without further purification