HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,4-Dioxane hydrochloride → HCID 55298731, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,4-Dioxane hydrochloride | HCID 20443148 | — |
| Reactant | HCID 59710395 | HCID 59710395 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 55298731 | HCID 55298731 | 147.1% |
Reaction Steps
1,1-Dimethylethyl(4E)-3-methyl-4-[(methyloxy)imino]-1-piperidinecarboxylate (197 mg) was dissolved in methanol, treated with 4.0 N HCl/dioxane (4 mL) and stirred overnight. The reaction was then concentrated to provide the product as a white solid (170 mg). The crude material was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07625909B2 |
| Source dataset | uspto-grants-2009_12 |
| ORD ID | ord-a99f0af5f4f14a0782c2824fd68a3fa1 |
| Source note | uspto-grants-2009_12 |