HRID1864517

反应详情

EQUATION

反应方程式

HRID 1864517 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

A solution of 1,1-dimethylethyl [1-(diphenylmethyl)-3-azetidinyl]carbamate in MeOH (10 mL) was treated with of 4.0 N HCl/dioxane (1 mL) and then reacted overnight with hydrogen gas at 50 psi. The reaction mixture was then filtered through a pad of Celite, concentrated and the crude residue was used without further purification.

WORKUP

后处理

  1. filtrationThe reaction mixture was then filtered through a pad of Celite
  2. concentrationconcentrated
  3. customthe crude residue was used without further purification