HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 66973356, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 66973000 | HCID 66973000 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 66973356 | HCID 66973356 | — |
Reaction Steps
A solution of methyl 1-[({1-[(tert-butoxycarbonyl)amino]-4,6-difluoro-2,3-dihydro-1H-inden-1-yl}methyl)amino]cyclopentanecarboxylate from Step G (753 mg, 1.77 mmol) in EtOAc (40 mL) at 0° C. was saturated with HCl (g). The reaction mixture was aged at 0° C. for 45 min then concentrated in vacuo to give the title compound. MS: m/z=325 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07625901B2 |
| Source dataset | uspto-grants-2009_12 |
| ORD ID | ord-155281df4ec84a1db4afeef6efeb96bf |
| Source note | uspto-grants-2009_12 |