HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethyl Sulfate → HCID 11392341, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethyl Sulfate | HCID 6497 | — |
| Reactant | HCID 11196840 | HCID 11196840 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 11392341 | HCID 11392341 | — |
Reaction Steps
Treat 3-phenylsulfanyl-1H-pyrrolo[3,2-b]pyridine-2-carboxylic acid methylamide Ia-33 (1.0 equiv) in DMF with dimethylsulfate (1.5 equiv) as described in General Synthetic Procedure V to provide Ia-29 as an ivory colored solid, MS Obs 298.09 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07626027B2 |
| Source dataset | uspto-grants-2009_12 |
| ORD ID | ord-1caa879758aa42a4b38751c5a2aee8fa |
| Source note | uspto-grants-2009_12 |