Hydrochloric Acid → HCID 67377193, compound

Participants

Reaction Steps

The product obtained in example 70 (1 gm; 2.58 mmol) was suspended in 10 ml ethanol and ethanolic hydrochloric acid (2.6 ml) was added at a temperature between 20-30° C. under stirring. To this solution, 20 ml ether was added after 30 minutes and the solid separated was filtered and dried under vacuum. Yield—0.86 gm (83%). m. p. (by DSC) 300° C., C21H26FN3O3.HCl, m/z 388 (M+1), [α]D25 value=+2750 (c=0.5, methanol).

Provenance & Evidence