Chloromethyl chloroformate → HCID 86604731, compound
Reaction equation
[Cl:1][CH2:2][O:3][C:4](Cl)=[O:5].[NH:7]([CH2:14][C:15]([O:17][CH2:18][CH3:19])=[O:16])[CH2:8][C:9]([O:11][CH2:12][CH3:13])=[O:10]>>[Cl:1][CH2:2][O:3][C:4]([N:7]([CH2:8][C:9]([O:11][CH2:12][CH3:13])=[O:10])[CH2:14][C:15]([O:17][CH2:18][CH3:19])=[O:16])=[O:5]Participants
3
Procedure
Using chloroformic acid chloromethyl ester and diethyl iminodiacetate as the raw materials, the same operation as the Example 101(1) gave the title compound as a crude product, and the crude product was used for the next reaction without further purification.
Sources & evidence
- ORD record
- ord-e61eeb2720af4474b5abbc8226bde829
- Source dataset
- uspto-grants-2009_12
- Patent number
- US07626042B2
Reaction notes
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