HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Methoxide → HCID 22015515, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Methoxide | HCID 10942334 | — |
| Reactant | HCID 22015518 | HCID 22015518 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 22015515 | HCID 22015515 | 82% |
Reaction Steps
A solution of tert-butyl 4-(6-amino-4-(2-furyl)-1H-pyrazolo[3,4-d]pyrimidine-1-ylmethyl)indole-1-carboxylate (92 mg, 0.17 mmol) in MeOH (3 mL) was treated with NaOMe (45 mg, 0.84 mmol), refluxed for 2 h, cooled, diluted with water (15 mL) and filtered to give the title compound (45 mg, 82%) as an off white powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07629349B2 |
| Source dataset | uspto-grants-2009_12 |
| ORD ID | ord-2bce082f53fb4087bfa7af5a76dea94f |
| Source note | uspto-grants-2009_12 |