HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86616406, compound → HCID 57974068, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86616406 | HCID 86616406 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 57974068 | HCID 57974068 | — |
Reaction Steps
A mixture of benzyl (4-ethyl-3-oxo-1-phenyl-2,5-diazabicyclo[2.2.2]oct-2-yl)acetate from Step A (127 mg, 0.336 mmol) and 10% Pd/C (20 mg) in MeOH (5 mL) was stirred under a balloon of hydrogen. The reaction mixture was filtered and concentrated in vacuo to give the title compound. MS: m/z=289 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07629338B2 |
| Source dataset | uspto-grants-2009_12 |
| ORD ID | ord-2c5967d849e74bd79269c9d2a8f4a054 |
| Source note | uspto-grants-2009_12 |