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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1866718Generated: November 1, 2026

HCID 86616406, compound → HCID 57974068, compound

https://huagongshe.com/reaction/1866718

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 86616406HCID 86616406—
ReactantHCID 178418361HCID 178418361—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
ProductHCID 57974068HCID 57974068—

Reaction Steps

A mixture of benzyl (4-ethyl-3-oxo-1-phenyl-2,5-diazabicyclo[2.2.2]oct-2-yl)acetate from Step A (127 mg, 0.336 mmol) and 10% Pd/C (20 mg) in MeOH (5 mL) was stirred under a balloon of hydrogen. The reaction mixture was filtered and concentrated in vacuo to give the title compound. MS: m/z=289 (M+1).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07629338B2
Source datasetuspto-grants-2009_12
ORD IDord-2c5967d849e74bd79269c9d2a8f4a054
Source noteuspto-grants-2009_12