HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 69056511, compound → HCID 69056714, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 69056511 | HCID 69056511 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | HCID 69056714 | HCID 69056714 | 68.3% |
Reaction Steps
According to the procedure of example 2, by hydrogenation of 1.00 g (4.80 mmol) of 2-(3′,3′-dimethylcyclohexyl)-2,5-dimethyl-2,5-dihydrofuran in the presence of 100 mg (0.0940 mmol) of 10% palladium on activated charcoal. Kugelrohr distillation furnished at 65-70° C./0.1 mbar 690 mg (68%) of the title compound as a colorless odoriferous liquid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07632790B2 |
| Source dataset | uspto-grants-2009_12 |
| ORD ID | ord-9d3ab117ded04cf6ab4c0cbe04039083 |
| Source note | uspto-grants-2009_12 |