Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1,4-Diazepan-5-one → 1-[(E)-3-(4-Chloro-3-fluoro-phenyl)-acryloyl]-[1,4]diazepan-5-one
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1,4-Diazepan-5-one | HCID 2737264 | — |
| 반응물 | 4-Chloro-3-fluorocinnamic acid | HCID 5708403 | — |
| 생성물 | 1-[(E)-3-(4-Chloro-3-fluoro-phenyl)-acryloyl]-[1,4]diazepan-5-one | HCID 68432166 | — |
반응 단계
In analogy to the procedure described for intermediate 1A, (E)-4-chloro-3-fluorocinnamic acid and 2,3,6,7-tetrahydro-(1H)-1,4-diazepin-5(4H)-one gave the title compound as white solid. MS: 297.3 (MH+).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07632829B2 |
| 출처 데이터셋 | uspto-grants-2009_12 |
| ORD ID | ord-a87af4bccd0a4ca19acc41560733e115 |
| 출처 메모 | uspto-grants-2009_12 |