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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1867388Generated: October 25, 2026

3,4-Dichlorocinnamic acid → (Rac)-1-[(e)-3-(3,4-dichloro-phenyl)-acryloyl]-3-methyl-[1,4]diazepan-5-one

https://huagongshe.com/reaction/1867388

Reaction equation

Participants

RoleNameHCIDCharge
Reactant3,4-Dichlorocinnamic acidHCID 688027—
Reactant3-Methyl-1,4-diazepan-5-oneHCID 68434036—
Product(Rac)-1-[(e)-3-(3,4-dichloro-phenyl)-acryloyl]-3-methyl-[1,4]diazepan-5-oneHCID 68435157—

Reaction Steps

In analogy to the procedure described in intermediate 1A, (E)-3,4-dichlorocinnamic acid and 3-methyl-[1,4]diazepan-5-one gave the title compound as a white solid. MS: 327.2 (MH+).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07632829B2
Source datasetuspto-grants-2009_12
ORD IDord-c9494c340a914e88a8a6d74f4a2e0309
Source noteuspto-grants-2009_12