Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 1867429생성일: 2026년 10월 25일
Sodium Iodide → 1-[(E)-3-(3,4-Dichloro-phenyl)-acryloyl]-4-(5-iodo-pentyl)-[1,4]diazepan-5-one
https://huagongshe.com/reaction/1867429
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Sodium Iodide | HCID 5238 | — |
| 반응물 | 4-(5-Chloro-pentyl)-1-[(E)-3-(3,4-dichloro-phenyl)-acryloyl]-[1,4]diazepan-5-one | HCID 68433224 | — |
| 생성물 | 1-[(E)-3-(3,4-Dichloro-phenyl)-acryloyl]-4-(5-iodo-pentyl)-[1,4]diazepan-5-one | HCID 68432952 | — |
반응 단계
In analogy to the procedure described in example 6D, 4-(5-chloro-pentyl)-1-[(E)-3-(3,4-dichloro-phenyl)-acryloyl]-[1,4]diazepan-5-one and sodium iodide were stirred at 90° C. for 20 h to give the title compound as orange oil. MS: 509.2 (MH+, 2Cl).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US07632829B2 |
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| 출처 데이터셋 | uspto-grants-2009_12 |
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| ORD ID | ord-a5843e680478422ea7d91c2d47df035c |
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| 출처 메모 | uspto-grants-2009_12 |
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