HCID 86604702, compound → HCID 86604701, compound

Participants

Reaction Steps

391 mg (1 mmol) (4-benzo[1,2,5]oxadiazol-5-yl-phenyl)-(2-fluoro-ethyl)-carbamic acid benzyl ester are hydrogenated in the presence of Pd/C, the reaction mixture filtered through celite and evaporated to dryness. The residues is column chromatographed (dichloromethane/petroleum ether 8:2) to yield the desired product as a yellow powder. MS(ES+): 258 (M+1).

Provenance & Evidence