HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl Glycolate → Ethyl [(phenoxycarbonyl)oxy]acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl Glycolate | HCID 12184 | — |
| Reactant | Phenyl chloroformate | HCID 15891 | — |
| Reactant | Diisopropylethylamine | HCID 81531 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | Ethyl [(phenoxycarbonyl)oxy]acetate | HCID 12094709 | — |
Reaction Steps
A solution of 25 g (240 mmol) of ethyl glycolate and 55 ml (315 mmol) of diisopropylethylamine in 500 ml of toluene is admixed slowly at ambient temperature with 32 ml (256 mmol) of phenyl chloroformate. Stirring is continued at ambient temperature for 2 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07632850B2 |
| Source dataset | uspto-grants-2009_12 |
| ORD ID | ord-c00dad19c4654875ac7fb37e6ac54edb |
| Source note | uspto-grants-2009_12 |